\u82b3\u9999\u80fa\u4e0e\u950c\u79bb\u5b50\u7edc\u5408\u7269<\/strong><\/a>\u200b\u5728\u7c89\u672b\u6d82\u6599\u4e2d\u7684\u6d88\u5149\u4f5c\u7528\u63a2\u7a76<\/p>\n\u514d\u8d23\u58f0\u660e\uff1a\u90e8\u5206\u8d44\u6599\u6765\u6e90\u4e8e\u7f51\u7edc\uff0c\u8f6c\u8f7d\u7684\u76ee\u7684\u5728\u4e8e\u4f20\u9012\u66f4\u591a\u4fe1\u606f\u53ca\u5206\u4eab\uff0c\u5e76\u4e0d\u610f\u5473\u7740\u8d5e\u540c\u5176\u89c2\u70b9\u6216\u8bc1\u5b9e\u5176\u771f\u5b9e\u6027\uff0c\u4e5f\u4e0d\u6784\u6210\u5176\u4ed6\u5efa\u8bae\u3002\u4ec5\u63d0\u4f9b\u4ea4\u6d41\u5e73\u53f0\uff0c\u4e0d\u4e3a\u5176\u7248\u6743\u8d1f\u8d23\u3002\u5982\u6d89\u53ca\u4fb5\u6743\uff0c\u8bf7\u8054\u7cfb\u6211\u4eec\u53ca\u65f6\u4fee\u6539\u6216\u5220\u9664\u3002<\/p>\n
<\/p>\n
\u6458\u8981\uff1a2-\u5def\u57fa\u5e76\u567b\u5511\u950c\uff08ZMBT\uff09\u5728\u7c89\u672b\u6d82\u6599\u7684\u6d88\u5149\u4f53\u7cfb\u4e2d\u5e94\u7528\u5e7f\u6cdb\uff0c\u672c\u6587\u5bf9\u5176\u6d88\u5149\u7684\u7ed3\u6784\u6a21\u578b\u63d0\u51fa\u5982\u4e0b\u5047\u8bbe\uff1a\u201c\u73af\u6c27\u6811\u8102\u56fa\u5316\u5242\uff0b\u950c\u79bb\u5b50\u201d\u7ed3\u6784\u6a21\u578b\u53ef\u7528\u4f5c\u73af\u6c27\u6811\u8102\u7c89\u672b\u6d82\u6599\u6d88\u5149\uff0c\u5e76\u6839\u636e\u8be5\u5047\u8bbe\u5408\u6210\u4e86\u4e24\u79cd\u82b3\u9999\u80fa4,4-\u4e8c\u6c28\u57fa\u7532\u70f7\uff08DDM\uff09\u30014,4-\u4e8c\u6c28\u57fa\u4e8c\u781c\uff08DDS\uff09\u4e0e\u6c2f\u5316\u950c\u7684\u7edc\u5408\u7269\uff0c\u5bf9\u6bd4\u4e86\u4e24\u79cd\u82b3\u9999\u80fa\u4ee5\u53ca\u76f8\u5e94\u7684\u950c\u76d0\u7edc\u5408\u7269\u4e0eZMBT\u7684\u6d88\u5149\u6548\u679c\u3002\u7ed3\u679c\u8868\u660e\u4e24\u79cd\u7edc\u5408\u7269\u5728\u7c89\u672b\u6d82\u6599\u4e2d\u5747\u5177\u6709\u4e0eZMBT\u7c7b\u4f3c\u7684\u6d88\u5149\u6548\u679c\uff0c\u4f46\u4e0e\u5176\u4ed6\u6d88\u5149\u7269\u8d28\u590d\u914d\u65e0\u6cd5\u5f97\u5230\u66f4\u4f4e\u7684\u6d82\u819c\u5149\u6cfd\u3002<\/p>\n
<\/p>\n
1 \u524d\u8a00<\/p>\n
\u4ee52-\u5def\u57fa\u5e76\u567b\u5511\u950c\uff08ZMBT\uff09\u4e3a\u57fa\u7840\u5efa\u7acb\u7684\u7c89\u672b\u6d82\u6599\u6d88\u5149\u4f53\u7cfb\u76ee\u524d\u5e94\u7528\u4e3a\u5e7f\u6cdb\uff1b\u8be5\u4f53\u7cfb\u6d88\u5149\u6548\u679c\u7a33\u5b9a\uff0c\u5149\u6cfd\u53ef\u8c03\u6027\u5f3a\uff0c\u540c\u65f6\u5177\u6709\u4f18\u5f02\u7684\u6297\u9ec4\u53d8\u6027\u80fd\uff0c\u4f46\u7c89\u672b\u6d82\u6599\u50a8\u5b58\u7a33\u5b9a\u6027\u6b20\u4f73\u3002ZMBT\u75312-\u5def\u57fa\u5e76\u567b\u5511\uff08MBT\uff09\u5728\u78b1\u6027\u6761\u4ef6\u4e0b\u4e0e\u950c\u79bb\u5b50\u590d\u5206\u89e3\u800c\u6210[1]\uff0c\u5176\u4e2dMBT\u53ef\u4ee5\u4e0e\u73af\u6c27\u57fa\u53d1\u751f\u5f00\u73af\u52a0\u6210\u53cd\u5e94[2]\uff0c\u53ef\u4f5c\u4e3a\u73af\u6811\u8102\u7684\u56fa\u5316\u5242\u6216\u56fa\u5316\u4fc3\u8fdb\u5242\u3002\u4e3a\u4e86\u63a2\u7a76\u82b3\u9999\u80fa\u950c\u76d0\u5bf9\u7c89\u672b\u6d82\u6599\u7684\u6d88\u5149\u673a\u7406\uff0c\u6211\u4eec\u63d0\u51fa\u5982\u4e0b\u5047\u8bbe\uff1a\u662f\u5426\u73af\u6c27\u6811\u8102\u7684\u56fa\u5316\u5242\u4e0e\u950c\u79bb\u5b50\u7ed3\u5408\u540e\u5c31\u6709\u53ef\u80fd\u8fbe\u5230\u6d88\u5149\u4f5c\u7528\uff1f<\/p>\n
<\/p>\n
\u57fa\u4e8e\u4e0a\u8ff0\u5047\u8bbe\uff0c\u6211\u4eec\u9009\u53d6\u4e24\u79cd\u82b3\u9999\u80fa\u7c7b\u73af\u6c27\u6811\u8102\u56fa\u5316\u5242\uff1a4,4-\u4e8c\u6c28\u57fa\u7532\u70f7\uff08DDM\uff09\u548c4,4-\u4e8c\u6c28\u57fa\u4e8c\u781c\uff08DDS\uff09\uff0c\u5176\u4e2dDDM\u53cd\u5e94\u6027\u8f83\u5f3a\uff0c\u53ef\u76f4\u63a5\u56fa\u5316\u7c89\u672b\u6d82\u6599\u7528E-12\u73af\u6c27\u6811\u8102\uff0cDDS\u6d3b\u6027\u8f83\u5f31\uff0c\u53ef\u4e0e\u6db2\u4f53\u73af\u6c27\u53cd\u5e94\uff0c\u800c\u4e14\u4e24\u79cd\u82b3\u9999\u80fa\u90fd\u80fd\u4e0e\u950c\u79bb\u5b50\u6709\u6548\u7edc\u5408[3]\u3002\u56e0\u6b64\u672c\u6587\u8bbe\u8ba1\u5408\u6210\u4e86\u4e0a\u8ff0\u4e24\u79cd\u73af\u6c27\u6811\u8102\u56fa\u5316\u5242\u4e0e\u950c\u79bb\u5b50\u7684\u7edc\u5408\u7269\uff08\u5982\u56fe1\u6240\u793a\uff09\uff0c\u5bf9\u6bd4\u4e86\u4e24\u79cd\u82b3\u80fa\u7c7b\u56fa\u5316\u5242\u4ee5\u53ca\u76f8\u5e94\u7684\u950c\u76d0\u7edc\u5408\u7269\u4e0e\u4f20\u7edf2-\u5def\u57fa\u5e76\u567b\u5511\u950c\u4f53\u7cfb\u7684\u6d88\u5149\u6548\u679c\u3002<\/p>\n
2 \u5b9e\u9a8c\u90e8\u5206<\/p>\n
2.1 \u539f\u6599<\/p>\n
\u6c2f\u5316\u950c\uff08\u5206\u6790\u7eaf\uff09\uff0c\u4e59\u9187\uff0895%\uff09\uff0cDDM\uff0cDDS\uff0cZMBT\uff0c\u4e8c\u7532\u57fa\u4e8c\u786b\u4ee3\u6c28\u57fa\u7532\u9178\u950c\uff08ZDEC\uff0c\u7194\u70b9250\u00b0C\uff09\uff0c\u73af\u6c27\u6811\u8102E-12\uff0c\u65b0\u4e2d\u6cd550\/50\u805a\u916fP5086\uff0c\u5b89\u5fbd\u795e\u525150\/50\u805a\u916fSJ3#B\uff0c\u80b2\u9716\u805a\u916fYL5050\uff0c\u94dd\u76d0\uff0c\u6d88\u5149\u94a1\uff0c\u589e\u5149\u5242\uff0c\u6d41\u5e73\u5242\uff0c\u5b89\u606f\u9999\uff0c\u70ad\u9ed1\u7b49\u5747\u4e3a\u5de5\u4e1a\u7ea7\u3002<\/p>\n
2.2 \u5b9e\u9a8c\u8bbe\u5907<\/p>\n
\u4e09\u53e3\u70e7\u74f6\uff08500mL\uff09\uff0c\u5e26\u78c1\u529b\u6405\u62cc\u6cb9\u6d74\u52a0\u70ed\u9505\uff0c\u62bd\u6ee4\u88c5\u7f6e\uff0c\u53cc\u87ba\u6746\u6324\u51fa\u673a\uff0c\u9ad8\u538b\u9759\u7535\u55b7\u6d82\u8bbe\u5907\uff0c\u6052\u6e29\u9f13\u98ce\u70d8\u7bb1\uff0c\u6d82\u819c\u6d4b\u539a\u4eea\u3001\u5149\u6cfd\u4eea\u3001\u6d82\u819c\u51b2\u51fb\u5668\u3001\u91d1\u76f8\u663e\u5fae\u955c\u7b49\u3002<\/p>\n
2.3 DDM\/\u950c\u79bb\u5b50\u7edc\u5408\u7269\u5236\u5907<\/p>\n
\u82b3\u9999\u80fa\/\u950c\u76d0\u7edc\u5408\u7269\u7684\u5408\u6210\u8fc7\u7a0b\u5982\u4e0b[4]\uff0c\u5728\u70e7\u74f6\u4e2d\u52a0\u516519.8 g DDM\u4e0e100 mL\u4e59\u9187\uff0c\u572860\u2103\u6cb9\u6d74\u4e2d\u6405\u62cc\u81f3\u5b8c\u5168\u6eb6\u89e3\uff0c\u5411\u6eb6\u6db2\u4e2d\u52a0\u516514g\u6c2f\u5316\u950c\uff0c\u7acb\u523b\u6790\u51fa\u5927\u91cf\u56fa\u4f53\uff0c\u7ee7\u7eed\u6405\u62cc\u53cd\u5e9430 min\u540e\u51b7\u5374\u3001\u62bd\u6ee4\u3001\u6d17\u6da4\uff0c50\u2103\u70d8\u7bb1\u5e72\u71e52h\u5f97\u523030 g\u6de1\u9ec4\u8272\u7c89\u672b\u72b6\u56fa\u4f53\uff0c\u5373DDM\/Zn2+\u7edc\u5408\u7269\uff0c\u4ea7\u738788.7%\uff0c\u7194\u70b9320 \u2103\u3002<\/p>\n
2.4 DDS\/\u950c\u79bb\u5b50\u7edc\u5408\u7269\u5236\u5907<\/p>\n
\u5728\u70e7\u74f6\u4e2d\u52a0\u516524.8 g DDS\u4e0e100 mL\u4e59\u9187\uff0c\u572860 \u2103\u6cb9\u6d74\u4e2d\u6405\u62cc\u81f3\u5b8c\u5168\u6eb6\u89e3\uff0c\u5411\u6eb6\u6db2\u4e2d\u52a0\u516514 g\u6c2f\u5316\u950c\uff0c\u6405\u62cc\u53cd\u5e942h\u540e\u51b7\u5374\u3001\u62bd\u6ee4\u3001\u6d17\u6da4\uff0c50\u2103\u70d8\u7bb1\u5e72\u71e52h\u5f9732 g\u767d\u8272\u7c89\u672b\u72b6\u56fa\u4f53\uff0c\u5373DDS\/Zn2+\u7edc\u5408\u7269\uff0c\u4ea7\u738782.3%\uff0c\u7194\u70b9315\u2103\u3002<\/p>\n
2.5 \u7c89\u672b\u6d82\u6599\u53ca\u6d82\u5c42\u5236\u5907<\/p>\n
\u5c06\u5b9e\u9a8c\u7528\u6811\u8102\uff0c\u56fa\u5316\u5242\u586b\u6599\u7b49\u6309\u914d\u65b9\u91cf\u5145\u5206\u6df7\u5408\u5747\u5300\uff0c\u7ecf\u8fc7\u878d\u5165\u6324\u51fa\u2192\u51b7\u5374\u538b\u7247\u2192\u7c89\u788e\u2192\u8fc7\u7b5b\u2192\u7c89\u672b\u6d82\u6599\uff0c\u7136\u540e\u7ecf\u8fc7\u9759\u7535\u55b7\u6d82\u5728\u9a6c\u53e3\u94c1\u677f\u4e0a\uff0c\u539a\u5ea6\u63a7\u5236\u572870~90 \u03bcm\uff0c\u7ecf200\u2103\/12 min\u56fa\u5316\u5f97\u5230\u6d82\u819c\u3002<\/p>\n
3 \u7ed3\u679c\u4e0e\u8ba8\u8bba<\/p>\n
3.1 \u56fa\u5316\u73af\u6c27\u6811\u8102\u6d88\u5149<\/p>\n
\u6839\u636e\u88681\u7684\u6570\u636e\uff0c\u56db\u79cd\u950c\u79bb\u5b50\u7edc\u5408\u7269\u5747\u53ef\u8f83\u597d\u5730\u56fa\u5316\u73af\u6c27\u6811\u8102\uff0c\u6d82\u819c\u51b2\u51fb\u6027\u80fd\u826f\u597d\uff1b\u4ece\u53ef\u770b\u51fa\uff0cZMBT\uff0cDDM\/Zn2+\uff0cDDS\/Zn2+\u56fa\u5316\u540e\u4ea7\u751f\u5e73\u6574\u7684\u6d88\u5149\u8868\u9762\uff0c\u5fae\u89c2\u7684\u8868\u9762\u5f62\u8c8c\u5f88\u63a5\u8fd1\uff0c\u7b26\u5408\u5047\u8bbe\u3002<\/p>\n
ZDEC\u4e0d\u662f\u73af\u6c27\u6811\u8102\u56fa\u5316\u5242\u4e0e\u950c\u79bb\u5b50\u7684\u7ed3\u5408\u800c\u6210\uff0c\u4e0d\u7b26\u5408\u201c\u73af\u6c27\u56fa\u5316\u5242\uff0b\u950c\u79bb\u5b50\u201d\u7ed3\u6784\u6a21\u578b\uff0c\u4e4b\u6240\u4ee5\u80fd\u56fa\u5316\u73af\u6c27\u6811\u8102\uff0c\u662f\u56e0\u4e3aZDEC\u4e2d\u7684\u950c\u79bb\u5b50\uff1b\u6c2f\u5316\u950c\u662f\u4e00\u79cd\u8def\u6613\u65af\u9178\uff0c\u672c\u8eab\u53ef\u4fc3\u8fdb\u73af\u6c27\u5f00\u73af\u53cd\u5e94\uff0c\u4f46\u53cd\u5e94\u901f\u5ea6\u8fc7\u5feb\u4e0d\u5b9c\u5355\u72ec\u4f7f\u7528[3]\uff0cZDEC\u4e2d\u7684\u914d\u4f53\u6539\u53d8\u4e86\u950c\u79bb\u5b50\u7684\u53cd\u5e94\u6027\u4f7fZDEC\u53ef\u56fa\u5316\u73af\u6c27\u6811\u8102\uff1b\u6d82\u819c\u8868\u9762\u5f62\u8c8c\u76b1\u7eb9\u7684\u539f\u56e0\u53ef\u80fd\u662f\u56fa\u5316\u53cd\u5e94\u901f\u5ea6\u8fc7\u5feb\uff1b\u800c\u6d88\u5149\u4f5c\u7528\u662f\u56e0\u6d82\u819c\u7684\u76b1\u7eb9\u6548\u679c\u4ea7\u751f\u7684\u3002<\/p>\n
ZMBT\uff0cDDM\/Zn2+\uff0cDDS\/Zn2+\u56fa\u5316\u73af\u6c27\u6811\u8102\u80f6\u5316\u65f6\u95f4\u5dee\u522b\u8f83\u5927\uff0c\u8fd9\u521a\u597d\u540c\u4e09\u4e2a\u914d\u4f53MBT\uff0cDDM\uff0cDDS\u4e0e\u73af\u6c27\u6811\u8102\u7684\u53cd\u5e94\u6027\u987a\u5e8f\u543b\u5408\uff1bDDS\u53cd\u5e94\u6027\u5f31\uff0c\u6240\u4ee5DDS\/Zn2+\u56fa\u5316\u73af\u6c27\u80f6\u5316\u65f6\u95f4\u957f\uff1bMBT\u53cd\u5e94\u6027\u5f3a\uff0cZMBT\u80f6\u5316\u65f6\u95f4\u77ed\u3002<\/p>\n
3.2 \u6df7\u5408\u4f53\u7cfb\u6d88\u5149<\/p>\n
\u6839\u636e\u88682\u4e2d\u7684\u6570\u636e\uff0cZMBT\uff0cDDM\/Zn2+\uff0cDDS\/Zn2+\u5728\u6df7\u5408\u4f53\u7cfb\u4e2d\u53ef\u5b9e\u73b0\u6709\u6548\u6d88\u5149\uff0c\u53ef\u964d\u4f4e10%\u5de6\u53f3\u7684\u5149\u6cfd\u4e14\u8868\u9762\u5e73\u6574\uff1b\u4ece\u56fe3\u663e\u5fae\u955c\u7167\u7247\u4e0a\u53ef\u4ee5\u76f4\u89c2\u7684\u770b\u51fa\u6765\uff1b\u7a7a\u767d\u7ec4(a)\u8868\u9762\u5f62\u8c8c\u8f83\u5e73\u6574\uff0c\u800cDDM(b)\u3001ZMBT(c)\u3001DDS(d)\u5747\u80fd\u6539\u53d8\u6d82\u819c\u8868\u9762\u7684\u5fae\u89c2\u7c97\u7cd9\u5ea6\uff0c\u4ea7\u751f\u66f4\u5bc6\u96c6\u66f4\u6df1\u7684\u201c\u5c0f\u5b54\u201d\uff0c\u4ece\u800c\u6d88\u5149\u3002\u56e0ZDEC\u4e0d\u7b26\u5408\u201c\u73af\u6c27\u56fa\u5316\u5242\uff0b\u950c\u79bb\u5b50\u201d\u7ed3\u6784\u6a21\u578b\uff0c\u6240\u4ee5\u4e0d\u80fd\u5728\u6df7\u5408\u4f53\u7cfb\u4ea7\u751f\u6d88\u5149\u4f5c\u7528\uff1b<\/p>\n
\u56e0\u4e3a\u950c\u79bb\u5b50\u5316\u5408\u7269\u53ef\u8ba4\u4e3a\u662f\u73af\u6c27\u6811\u8102\u7684\u534f\u540c\u56fa\u5316\u5242\uff0c\u5176\u7194\u70b9\u8f83\u9ad8\uff0c\u4ece\u800c\u5ef6\u957f\u4e86\u73af\u6c27\u6811\u8102\u7684\u56fa\u5316\u65f6\u95f4\uff1b\u6240\u4ee5ZMBT\uff0cDDM\/Zn2+\uff0cDDS\/Zn2+\u52a0\u5165\u6df7\u5408\u4f53\u7cfb\u914d\u65b9\u4e2d\uff0c\u80f6\u5316\u65f6\u95f4\u5747\u9ad8\u4e8e\u5176\u5bf9\u5e94\u7684\u7a7a\u767d\u7ec4\u3002\u5176\u4e2dZMBT\u5bf9\u56fa\u5316\u65f6\u95f4\u7684\u5f71\u54cd\u5f31\uff0c\u800cDDS\/Zn2+\u5bf9\u56fa\u5316\u65f6\u95f4\u7684\u5f71\u54cd\u660e\u663e\uff0c\u4ece\u7a7a\u767d\u7ec4\u7684225 s\u5ef6\u957f\u5230300 s\uff1b\u80f6\u5316\u65f6\u95f4\u7684\u5dee\u5f02\u662f\u7531MBT\uff0cDDM\uff0cDDS\u4e0e\u73af\u6c27\u57fa\u53cd\u5e94\u901f\u7387\u5dee\u522b\u6240\u81f4\uff0c\u8fd9\u53ef\u80fd\u5c06\u7ec8\u5f71\u54cd\u950c\u79bb\u5b50\u5316\u5408\u7269\u7684\u590d\u914d\u6d88\u5149\u6027\u80fd\u3002<\/p>\n
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4 \u7ed3\u8bed<\/p>\n
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